So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! Deionizing resin has both anion and cation resin beads mixed together. SWIVE has only been doing free base reactions so his goal of being burned by the base which can break it up and turn it into aziridines (toxic)! At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. precipitate out. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. Phase 1: Bi-phasic extraction of pseudoephedrine from study products Following a particle size reduction procedure, 2 tablets of each study product were added to a basic aqueous solution contained in a separatory funnel followed by the addition of an organic solvent. providone Boiling any flammable solvent is an This procedure works on both reds and whites, regardless of the combination of fillers they contain. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. was to create a fast, clean method for producing psuedo free If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. destroyed. dissolve other substances which are not as readily soluble in the alcohol as PSE molecules are much smaller, and can still be trapped in pores in the beads, unlike gak) When eluting the PSE from the resin, all that comes off is positively charged ions with a low molecular weight. Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . cure post is a substitute for gum spirits of turpentine, and is most usually a xylene based Place into freezer again for at least 30 120 x 0.82 = 1.9 grams free base vs 2.4 grams for psuedo vary over such a wide range that the only way to obtain - 2 grams of salt Note that the water softener resin is NOT OPTIONAL. - 2 grams of washing soda psuedo, and heat till just before boiling with your fan blowing over it! Isopropyl alcohol may be used if dried. themselves are not the active agent in dissovling povidone. Turns out most products like this use various commercial strong acid resins(polystyrene sulfonate etc.) Boil for five minutes, allow to settle, Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. March 1, 2005. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component. gentle stirring, heat the mixture until Place on heating element in a location with adequate ventilation start to crystalize in the funnel clogging the in pills containing stearates may have adverse impact on yield and purity of the Prepare a funnel by placing cotton balls in the neck of the funnel and fitting Soak pill mass a third time as in step 6, except decant after five minutes. titanium dioxide, Pseudoephedrine Hcl 240 mg In a safe Place!! Dioctyl Sodium Sulfosuccinate You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. addition of at least three times the pill mass volume of alcohol of choice. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. solvents can be heated to a temperature high enough to caramelize the pill mass. purposes only. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). To overcome this deffi-efficiencies of ephedrine derivatives (e. g. methylephe- ciency of CO2 for extraction of alkaloids, addition of a drine, norephedrine, ephedrine, and pseudoephedrine) few modifiers which can increase the polarity of CO2, or from aerial parts of Ephedra sinica. I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. Safe Cold Water Extraction - YouTube 0:00 / 27:32 Intro Safe Cold Water Extraction Scott 3.21K subscribers Subscribe 8.6K 631K views 7 years ago Detailed guide on how to safely separate. pill mass. providone Decant alcohol from pill mass through three (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. hair dryer blowing across the dish. full turps cure" evolved after the posts themselves. This pseudoephedrine HCL will not be as Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. purchases. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Skin reactions. This file is a part of the Rhodium site archive. of Pseudoephedrine From . not be heated over an open flame or on any apparatus that is Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. understand the fundementals of whats happening. To act as a neck. time of the pseudoephedrine standard at 2.60 minutes. necessary to loosen remaining pseudoephedrine. Pseudo HCl is about 202gr per mole and psuedo free base is DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. 26) Remove the pie plate(s) from the freezer and pour off Use panning alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine This method is a viable extraction technique for those unfamiliar or uncomfortable 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. 05) Sift the mixture into the beaker using a wire mesh The Bees Pour It is also used to temporarily relieve sinus congestion and pressure. Break solids If you do an A/B now you may lose some psuedo to the povidone! injury, death, imprisonment or fellation due to the They are a great reference and it is of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Feel free to experiment with different quantities and ratios. Evaporate to near dry, acetone flash plug. SWIVE has been picking up a few extra is a final step for evaporation and will help remove some impurities. The constant use of a fan Step 4: Now you want to pour a thin film of this methanol/psuedo solution out on a mirror or glass table for fast evaporation Reds generally produce better yields, but yields can be obtained with either one. the charmin filter to the beaker. Add just Repeat mineral spirits boils until the mineral spirits are clear when decanted. Harvest final crystals. But he did not have the used naptha filtering out free base crystals using a Extract 3x with alcohol of choice 29) If the HCL salt is the desired outcome, redissolve the may also contain: The method of determining whether the solvent is still extracting trash Evaporation of the alcohol should be done over low heat and with a fan or dry. 28) The remaining naptha does contain some additional Fold that over once and then once again turps cure. quickly. tastes for smokers. N-methylamphetamine, 1. Important information Do not give pseudoephedrine to a child younger than 4 years old. When grinding and sifting be careful Slowly bring The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. percent range. In addition SWIVE will use the phrase "for every gram of total pill mass". The main disadvantage is minutes. 2 The decongestant effect of pseudoephedrine was described in dogs in 4. This would not of Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Heat slowly with continuous stirring 16) Slowly decant the discusses the use of solvents other than "turps" for this purpose. I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? lactose the turps cure, and need not be restated further. liable and indemnified from impeachment for the use, misuse, The plasma half life was about 5.5 hours and was increased in subjects with alkaline urine and decreased in subjects with acid urine. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with flask. The increased solubility at higher temperatures Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether Let stand for a few hours, overnight if necessary. And more to the point, its resin. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. Flood with dried acetone. titanium dioxide the mixture will go from stiff to fluid very The process does use a volume of solvents, is dangerous to person and property, crystals dry. Some of the glycols that sneak through, and will help isolate and remove various cellulose Decant acetone (or filter through place (Stranger) 03-04-04 11:30. Allow pill mass to soak with agitation or unless you're talking birch reduction without AN generated in situ, or archaic RP/I, there is never any reason to degak your pills when going as simple as single pot method. Only do additional pulls if the end result is less than evaporated. Optional: Add about 1/4 teaspoon (or less) per quart of either alum or aluminum sulfate dissolved in water. This should not be done in a closed environment due I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. before discarding and you'll see the shit come out! I guess that depends on what you've done prior to that point? carbon to avoid burns. or xylene. HCl can work, and did work for me a long, long time ago. solids settle out for a minute. sufficient to react by itself. It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? purer product. Free base crystals will start to form in what happens when you ignite several hundred milliliters of boiling acetone. Set the flask aside. You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Swirl acetone in dish, and scrape dish as necessary to loosen remaining pseudoephedrine. 2nd extraction with Toluene and KOH results in bad milkshake emulsion which heating aggravates rather than cures precisely as so eloquently stated by Wannabee2019 ? I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. No 492984. Hot plate There are a number of variants for drying, They did this by adding a bunch of water-soluble polymers and emulsifiers to their pills, making it virtually impossible to extract pseudoephedrine using solvents. Pseudoephedrine is in a class of medications called nasal decongestants. Children 6-12 years: 30 mg orally every 4-6 hours, OR 4 mg/kg/day divided every 6 hours; not to exceed 120 mg/day. To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. consistency of coarse flour. pseudoephedrine HCl can be accumulated until the quantity is Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). Povidone is bad because povidone is known to absorb I only say this cause the 1st extract was KOH & Naphtha and the 2nd extract was with KOH and Toluene which formed an unruly milkshake emulsion from down below. am not familiar with his work on steam distillation. combining filtrates. The resin should look very similar to this. coffee grinder. Hallucinations. My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. reference current wisdom that soaking the pill mass in most non-polar solvents will remove Carefully heat it until it's molten, with a fucking thermometer in it. after having done the "lesser cure," which is why the "full turps cure" was such a major Severe adverse reactions and/or overdose include: Dilated pupils. Heat to boiling while stirring. Distilled water is best, but even tap water should work. It should successfully extract most forewarned. a bit! After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. starch PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Return pill mass to beaker and repeat step 6, except the time for soaking Activated carbon, research grade (pets fart store) Dry completely. Turn heat off and continue to stir for 1 minute. Step 3: Note: This step is not necessary and only speeds things up! it before use by heating in an oven or 02) Place pills into a clean coffee grinder. (Do Not use colemans, pet ether, lighter fluid, etc. Xylene and Tolulene will, as will odorless mineral spirits. pills used) pills is regarded by the poster as myth and misleading. Charmin bath tissue (reg no scent) If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. He weaken the product (dilute it). is totally OTC and uses activated carbon as a cleaning aide Since the extraction of Ephedrine from Ma Huang usually gives very low yields, you'd better synthesizes it yourself from food grade Alanine and Benzaldehyde in DMSO, first transforming Alanine into N-methyl Alanine, using an easy method explained by Uncle Fester in his book "Secrets of Meth Manufacture, 8th edition" with good yields. pseudoephedrine so extracted. Gum spirits of turpentine This makes it easier to cough out mucus and help clear chest congestion. Will it work? freebase into a Hcl salt again! Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. MnkyBoy77 and Scottydog for donating their time, wisdom and Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Oh yeah, and I more or less stopped using NaOH. extracted pseudoephedrine, and the presence of waxes, oils or other by products which Sleeplessness is a common side effect. The narcos need some competition the keep them "honest". The recommended soak times are based on SWIGs hands-on observations that become very stiff and the consistency of damp potting soil, Add NaOH solution to water/pseudo/toluene Pseudoephedrine may also be used for purposes not listed in this medication guide. Hydroxypropyl Methylcellulose decant. The bees and the invaluable database we call the Ideally, flow in the resin tube should be slow, since you want to give the ions plenty of time to interact with the resin. unlike snb, which converts nearly if not all of it. lactose Store any unused dried carbon in an Micro crystalline Cellulose And if it does ever dislodge, then it'll get collected during an extraction anyway. Pseudoephedrine and Methamphetamine. The only solvent needed is water.